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   Syllabus
B.Sc.-Chemistry
B.Sc.-1-Chemistry
Sr.
Name of the PapersTheoretical/Practical/
Viva-voce/AssignmentMaximum MarksDuration
(hours)1.Inorganic ChemistryTheoretical503.002.Organic ChemistryTheoretical503.003Physical ChemistryTheoretical503.004.PracticalPractical50                                                          Total Marks = 200B.Sc-2-Chemistry 
Sr.
Name of the PapersTheoretical/Practical/
Viva-voce/AssignmentMaximum MarksDuration
(hours)1.Inorganic ChemistryTheoretical503.002.Organic ChemistryTheoretical503.003Physical ChemistryTheoretical503.004.PracticalPractical50                                                         Total Marks =200B.Sc.-3-Chemistry
Sr.
Name of the PapersTheoretical/Practical/
Viva-voce/AssignmentMaximum MarksDuration
(hours)1.Inorganic ChemistryTheoretical753.002.Organic ChemistryTheoretical753.003Physical ChemistryTheoretical753.004.PracticalPractical75                                                         Total Marks =300
B.Sc.-1
 Chemistry 
Paper-I
M.M. 50                                                                                                                        Duration-3.00 hours
Unit-I
Inorganic Chemistry 
A. Atomic Structure
			Idea of de-Brogiie matter waves, Heisenberg uncertainty principle, atomic orbitals, Schrodinger wave equation, significance of (( and (2, quantum numbers, radial and angular wave functions and probability distribution curves, shapes of s, p, d, orbitals, Aufbauand Pauli exclusion principles, Hund's multiplicity rule, Electronic configurations of the elements, effective nuclear charge.
B. Periodic Properties
			Atomic and ionic radii, ionization energy, electron affinity and electronegativity-definition, methods of determination or evaluation, trends in periodic table and applications in predicting and explaining the chemical behaviour.
Unit-II
Chemical Bonding
(A) Covalent Bond
Valence bond theory and its limitations, directional characteristics of covalent bond, various types of hybridization and shapes of simple inorganic molecules and ions, valence shall electron pair repulsion (VSEPR) theory to NH3, H3O+, SF4, CIF3, ICI"2 and H2O, MO theory, homo nuclear and hetero nuclear (CO and NO) diatomic molecules, multicenter bonding in electron deficient molecules, bond strength and bond energy, percentage ionic character from dipole moment and electro-negativity difference.
(B) Ionic Solids - Ionic structures, radius ratio effect and coordination number, limitation of radius ratio rule, lattice defects, semiconductors, lattice energy and Born-Haber cycle, salvation energy and solubility of ionic solids, polarizing power and Polaris ability of ions, Fajan's rule, Metallic bond-free electron, valence bond and band theories.
(C Weak Interactions-Hydrogen bonding, Vander Waals forces.
Unit-III
 (A).  S-Block Elements
	Comparative study, diagonal relationship, salient features of hydrides, solvation and
	complexation tendencies including their function in biosystems, an introduction to alkyls
	and aryls.
 (B). Chemistry of Noble Gasses
	Chemical properties of the noble gases, chemistry of xenon, structure and M bonding in
	xenon compounds.
Unit-IV
	P-Block Elements
	Comparative study (including diagonal relationship) of groups 13-17 elements, compounds  like  hydrides,  oxides,  oxyacids  and  halides  of group  13-16, hydrides  of  boron-diborane  and   higher  boranes,   borazine,   borohydrides, fullerenes, carbides, fluorocarbons, silicates (structural principle), tetrasulphur tetra nitride, basic properties of halogens, interhalogens and polyhalides.

B.Sc.-1 
Chemistry 
Paper-II
M.M. 50                                                                                                                        Duration-3.00 hours
Unit-I
	Organic Chemistry 
	A.  Structure and Bonding
	Hybridization, bond lengths and bond angles, bond energy, localized and delocalized chemical bonding, van der Waals interactions, inclusion compounds, clatherates, charge transfer complexes, resonance, hyperconjugation, aromaticity, inductive and field effects, hydrogen bonding.
	B. Mechanism of Organic Reactions
	Curved arrow notation, drawing electron movements with arrows, half-headed and double-headed arrows, homolytic and heterolytic bond fission. Types of reagents - electrophiles and nucleophiles, Types of organic reactions, Energy considerations.
	Reactive intermediates - Carbocations, carbanions, free radicals, carbenes, arynes and nitrenes (with examples). Assigning formal charges on intermediates and other ionic species.
	Methods of determination of reaction mechanism (product analysis, intermediates, isotope effects, kinetic and stereochemical studies).
	C. Alkanes and Cycloalkanes
	IUPAC nomenclature of branched and unbranched alkanes, the alkyl group, classification of carbon atom in alkanes, Isomerism in alkanes, sources, methods of formation (with special reference to Wurtz reaction, Kolbe reaction, Corey-House reaction and decarboxylation of carboxylic acids), physical properties and chemical reactions of alkanes, Mechanism of free radical halogenation of alkanes orientation, reactivity and selectivity.
	Cycloalkanes - Nomenclature, methods of formation, chemical reactions, Baeyer's strain theory and its limitations. Ring strain in small rings (cyclopropane and cyclobutane), theory of strain less rings. The case of cyclopropane ring, banana bonds.
Unit-II
        	 Stereochemistry of Organic Compounds
	Concept of isomerism, Types of isomerism;
	Optical isomerism - elements of symmetry, molecular chirality, enantiomers, stereogenic center, optical activity, properties of enantiomers, chiral and achiral molecules with two stereogenic centers, disasteromers, -three and erythro diastereomers, meso compounds, resolution of enantiomer, inversion, retention and recemization.
	Relative and absolute configuration, sequence rules, D & L and R & S systems of nomenclature.
	Geometric isomerism - determination of configuration of geometric isomers, E & Z system of nomenclature, geometric isomerism in oximes and alicyclic compounds.
	Conformational isomerism - conformational analysis of ethane and n-butane; conformations of cyclohexane, axial and equatorial bonds, conformation of mono substituted cyclohexane derivatives, Newman projection and Sawhorse formulae, Fischer and flying wedge formulae, Difference between configuration and conformation.
Unit-III
       	Alkenes, Cycloalkenes, Dienes and Alkynes
	Nomenclature of alkenes, methods of formation, mechanisms of dehydration of alcohols and dehydrohalogenation of alkyl halides, regioselectivity in alcohol dehydration, The Saytzeff rule, Hofmann elimination, physical properties and relative stabilities of alkenes.
	Chemical reactions of alkenes - mechanism involved in hydrogenation, electrophilic and free radical additions, Markownikoffs rule, hydroboration-oxidation, oxymercuration-reduction. Epoxidation, ozonolysis, hydration, hydroxylation and oxidation with KMnO4, Polymerization of alkenes, Substitution at the allylic and vinylic positions of alkenes, Industrial applications of ethylene and propene.
	Methods of formation, conformation and chemical reactions of cycloalkenes; Nomenclature and classification of dienes  isolated, conjugated and cumulated dienes, Structure of allenes and butadiene, methods of formation, polymerization, chemical reaction -1,2 and 1, 4 additions, Diels-Alder reaction. Nomenclature, structure and bonding in alkynes, Methods of formation, Chemical reactions of alkynes, acidity of alkynes, Mechanism of electrophilic and nucleophilic addition reactions, hydroboration-oxidation, metal-ammonia reductions, oxidation and polymerization.
Unit-IV
	A. Arenes and Aromaticity
	Nomenclature of benzene derivatives, The aryl group, Aromatic nucleus and side chain,  Structure of benzene; molecular formula and kekule structure, stability and carbon-carbon bond lengths of benzene, resonance structure, MO picture.
	Aromaticity The Huckle rule, aromatic ions.
	Aromatic electrophilic substitution - general pattern of the mechanism, role of ( & ( complexes, Mechanism of   nitration,   halogenation,   sulphonation, mercuration and Friedel-Crafts reaction. Energy profile diagrams. Activating and  deactivating  substituents, orientation and  ortho/para  ratio,  Side chain reactions of benzene derivatives, Birch reduction; Methods     of     formation     and     chemical     reactions     of     alkylbenzenes, alkynylbenzenes and biphenyl, naphthalene and Anthracene.
	B. Alkyl and Aryl Halides
	Nomenclature and classes of alkyl halides, methods of formation, chemical reactions, Mechanisms of nucleophilic substitution reactions of alkyl halides, SN2 and SN1 reactions with energy profile diagrams; Polyhalogen compounds  Chloroform, carbon tetrachloride; Methods of formation of aryl halides, nuclear and side chain reactions; The    addition-elimination    and    the    elimination-addition    mechanism    of nucleophilc aromatic substitution reactions;
	Relative reactivities of alkyl halides vs allyl, vinyl and aryl halides, Synthesis and uses of DDT and BHC.

B.Sc-1
Chemistry 
Paper-Ill
Physical Chemistry 
M.M. 50                                                                                                                        Duration-3.00 hours
Unit-I
I. Mathematical Concepts and Computers
(A)  Mathematical Concepts
	Logarithmic relations, curve sketching, linear graphs and calculation of slopes, differentiation of functions like kx, ex, Xn, sin x, log x; maxima and minima, partial differentiation and reciprocity relations, Integration of some useful/relevant functions; permutations and combinations, Factorials, Probability.
	(B) Computers
	General introduction to computers, different components of a computer, hardware and software, input-output devices; binary - numbers and arithmetic's; introduction to computer languages, programming, operating systems.


Unit-II
	A. Gaseous States
	Postulates of kinetic theory of gases, deviation from ideal behaviour, Vander Waals equation of state;
	Critical Phenomena  PV isotherms of real gases, continuity of states, the isotherms of vander Waals equation, relationship between critical constants and vander Waals constants, the iaw of corresponding states, reduced equation of state.
	Molecular velocities  Root mean square, average and most probable velocities, Qualitative discussion of the Maxwell's distribution of molecular velocities, collision number, mean free path and collision diameter, Liquefaction of gases (based on Joule -Thomson effect).
	B.  Liquid State
	Intermoiecular forces, structure of liquids (a qualitative description).
	Structural differences between solids, liquids and gases;
	Liquid crystals Differences between liquid crystals, solid and liquid, Classification, structure of nematic and cholestric phases, Thermbgraphy and seven segment cells.
Unit-III
	A.  Solid States
	Definition of space lattice, unit cell;
	Laws of crystallography - (i) Law of constancy of interfacial angles, (ii) Law of rational of indices (iii) Law of symmetry, Symmetry elements in crystals.
	X-ray diffraction by crystals, Derivation of Bragg�s equation, Determination of crystal structure of NaCI, KCI and CsCl, Laue's method and powder method.
	B. Colloidal States
	Definition of colloids, classification of colloids;
	Solids in liquids (sols) properties - kinetic, optical and electrical; stability of colloids, protective action, Hardy-Schulze law, gold number.
	Liquids in liquids (emulsions) types of emulsions, preparation, Emulsifier,
	Liquids in solids (gels)  classification, preparation and properties, inhibition, general application of colloids, colloidal electrolytes.

Unit-IV
	A. Chemical Kinetics and Catalysis
	Chemical kinetics and its scope, rate of a reaction, factors influencing the rate of a reaction - concentration, temperature, pressure, solvent, light, catalyst, concentration dependence of rates, mathematical characteristics of simple chemical reactions - zero order, first order, second order, pseudo order, half life and mean life, Determination of the order of reaction - differential method, method of integration, method of half life period and isolation method.
	Radioactive decay as a first order phenomenon;
	Experimental methods of chemical kinetics conductometric, potentiometric, optical methods, polarimetry and spectrophotometer.
	Theories of chemical kinetics effect of temperature on rate of reaction, Arrhenius equation, concept of activation energy.
	Simple collision theory based on hard sphere model, transition state theory (equilibrium hypothesis), Expression for the rate constant based on equilibrium constant and thermodynamic aspects.
	B. Catalysis, characteristics of catalysed reactions, classification of catalysis homogeneous and heterogeneous catalysis, enzyme catalysis, misccllaneous examples.

B.Sc.1
Chemistry 
PRACTICAL
 180 hours (6 hours/week)
M.M. 50                                                                                                                        
Inorganic Chemistry 
Semi micro Analysis -caption analysis, separation and identification of ions from
Grops I, II, III, IV, V and VI, Anion analysis.					                   20
Organic Chemistry 
Laboratory techniques;
Calibration of Thermometer.							                   10
80-82� (Naphthalene), 113.5-114� (Acetanilide)
132.5-133� (Urea), 100� (Distilled Water) 
Determination of melting point
Naphthalene 80-82�, Benzolic acid 121.5-122�
Urea 1 32.5-1 33�, Succinic acid 184.5-185�
Cinnamicacid 132.5-133�, Sallicylic acid 157.5-158�
Acetanilide 113.5 114� m-Dinitrobenzene 90�
p-Dichlorobenzene 52�, Aspirin 135� 
Determination of boiling point 
Ethanol 78�, Cyclohexane 81 .4�, Toluene 1 10.6�, Benzene 80� 
Mixed melting point determination
Urea-Cinnamicacid mixture of various compositions (14, 11, 41) 
Distillation
Simple distillation of ethanol-water mixture using water condenser,
Distillation of nitrobenzene and aniline using air condenser 
Crystallization 
Concept of induction of crystallization,
Phthalic acid from hot water (using fluted filter paper and steamless funnel)
Acetanilide from boiling water Naphthalene from ethanol Benzoic acid from water 
Decolorisation and crystallization using charcoal
Decolorsation of brown sugar (sucrose) with animal charcoal using gravity filtration.
Crystallization and decolorisation of impure naphthalene (100g of naphthalene mixes with 0.3 g of Congo Red using 1g decolorizing carbon) from ethanol.
Sublimation (Siple and Vacuum)
Camphor, Naphthalene, Phthalic acid and succinic acid. 
Qualitative Analysis-
Detection of extra elements (N, S and halogens) and functional groups (phenolic, carboxylic, carbonyl, esters, carbohydrates, amines, amides, nitro and anilide) in simple organic compounds.
Physical Chemistry 
 10
Chemical Kinetics
1.    To determine the specific reaction rate of the hydrolysis of methyl acetate/ethyl acetate catalyzed by hydrogen ions at rooms temperature.
2.        To study the effect of acid strength on the hydrolysis of an ester.
3.      To compare the strengths of HCI and H2SO4 by studying the kinetics of hydrolysis of ethyl acetate.
4.        To study kinetics of the reaction rate of decomposition of iodide by H2O2.
Distribution Law
1 .       To study the distribution of iodine between water and CCI4.
2.        To study the distribution of benzoic acid between benzene and water.
Colloids
1.        To prepare arsenious sulphide sol and compare the precipitating power of mono-, bi- and
	trivalent cations.
Viscosity, Surface Tension
1.	To determine the percentage composition of a giv mixture (non interacting systems) by viscosity method. 
2.	To   determine   the   viscosity   of   amyl   alcohol   in   water   at   different
,          concentration and calculate the excess viscosity of these solutions. Vs.   
3.	To determine the percentage composition of a given binary mixture by surface tension method (acetone & ethyl methyl ketone).
Viva-voce � 05
Practical record � 05
B.Sc.-2 
Chemistry 
Paper-I 
Inorganic Chemistry 
M.M. 50                                                                                                                         Duration-3.00 hours
Unit-I
          A.  Chemistry of Elements of First Transition Series
	Characteristic properties of d-block elements.
	Binary compounds (hydrides, carbides and oxides) of the elements of the first 	transition series and complexes with respect to relative stability of their oxidation 	states, 	coordination number and geometry.
         B. Chemistry of Elements of Second and Third Transition Series
	General characteristics, comparative treatment of Zr/Hf, Nb/Ta, Mo/W in respect of 	ionic radii, oxidation states, magnetic behavior, spectral properties and 	stereochemistry.
Unit-II
	Coordination Compounds
	Werner's coordination theory and its experimental verification, effective atomic 	number concept, chelates, nomenclature of coordination compounds, isomerism in 	coordination compounds, valence bond theory of transition metal complexes.
Unit-III
             A.  Chemistry of Lanthanide tiements
	Electronic structure, oxidation states and ionic radii and lanthanide contraction, 	complex formation, occurrence and isolation, ceric ammonium sulphate and its 	analytical uses.
	B.  Chemistry of Actinides -
	Electronic configuration, oxidation states and magnetic properties, chemistry of 	separation of Np, Pu and Am from U.
Unit-IV
            A.   Oxidation and Reduction
	Electrode   potential,   electrochemical  series  and   its  applications,   Principles involved 	in the extraction of the elements. 
          B.     Acids and Bases
	Arrhenius, Bronsted-Lowry, the Lux-Flood, solvent system and Lewis concept                                    	of acids and bases.
	C.    Non-aqueous Solvents
	Physical   properties   of  a   solvent,   types   of  solvents   and   their  general 	characteristics, Reactions in non-aqueous solvents with reference to liquid NH3
	and Liquid SO2
B.Sc. -2
Chemistry 
Paper-II 
Organic Chemistry 
M.M. 50                                                                                                                       Duration-3.00 hours
Unit-I
          I.  Electromagnetic Spectrum Absorption Spectra
	Ultraviolet (UV) absorption spectroscopy - absorption laws (Beer-Lambert law); molar 	absroptivity, presentation and analysis of UV spectra, types of electronic transitions, 	effect of conjugation. Concept of chromophore and auxochrome, Bathochromic, 	hypsochromic, hyperchromic and hypochromic shifts. U.V. spectra of conjugated enes 	and enones.
	Infrared (l.R.) absorption spectroscopy - molecular vibrations, Hooke's law, selection 	rules, intensity and position of l.R. bands, measurement of l.R. spectrum, fingerprint 	region, characteristic absorptions of various functional groups and interpretation of l.R. 	spectra of simple organic compounds.
Unit-II
	A.  Alcohols 
	Classification and nomenclature,
	Monohydric alcohols - nomenclature, methods of formation by reduction of
	Aldehydes,
	Ketones,
	Carboxylic acids and Esters, Hydrogen bonding, Acidic nature, Reactions of alcohols'. 	Dihydri calcohols Nomenclature, methods of formation, chemical reactions of vicinal 	glycols, oxidative   cleavage   [Pb(OAc)4   and    HIO4] and pinacol-pinacolone 	rearrangement.Trihydric alcohols- nomenclature, methods of formation, chemical reactions 	of glycerol.
	B. Phenols 
	Nomenclature, structure and bonding, preparation of phenols, physical properties and 	acidic character, Comparative acidic strengths of alcohols and phenols, resonance 	stabilization of phenoxide ion. Reactions of phenols -electrophilic aromatic substitution, 	acylation and carboxylation. Mechanism of Fries rearrangement, Claisen rearrangement, 	Gatterman synthesis, Hauben-Hoesch reaction, Lederer-Manasse reaction and Reimer-	Tiemann reaction.
Unit-III
            A. Ethers and Epoxides
	Nomenclature of ethers and methods of their formation, physical properties, Chemical 	reactions - cleavage and autoxidation, Ziesel's method. Synthesis of epoxides, Acid and 	base-catalyzed ring opening of epoxides, orientation of epoxide ring opening, reactions of 	Grignard and organolithium reagents with epoxides.
	B. Aldehydes and Ketones
	Nomenclature and structure of the carbonyl groups, synthesis of aldehydes and ketones 	with particular reference to the synthesis of aldehydes from acid chlorides, synthesis of 	aldehydes and ketones uses 1, 3-dithianes, synthesis of ketones from nitriles and from 	carboxylic acids, Physical properties.
Mechanism of nucleophillic additions to carbonyl group with particular emphasis on         benzoin, aldol, Perkin and Knoevenagel condensations, Condensation with ammonia and its derivatives, Wittig reaction, Mannich reaction.
Use of acetals as protecting group, Oxidation of aldehydes, Baeyer-Villiger oxidation of Ketones, Cannizzaro reaction, MPV, Clemmensen, Wolff-Kishner, LiAIH4 and NaBH4 reductions. Halogenation of enolizable ketones. An introduction to (, ( unsaturated aldehydes and Ketones.
Unit-IV
         A.   Carboxylic Acids
	Nomenclature, structure and bonding, physical properties, acidity of carboxylic acids,
	effects of substituents on acid strength, Preparation of carboxylic acids, Reactions of
          carboxylic acids,
	Hell-Volhard-Zelinsky reaction, Synthesis of acid chlorides, esters and amides, Reduction of carboxylic acids, Mechanism of decarboxylation.
         Methods of formation and chemical reactions of halo acids, Hydroxy acids;m malic,
	tartaric and citric acids.
	Methods of formation and chemical reactions of unsaturated monocarboxylic
	acids.
	Dicarboxylic acids methods of formation and effect of heat and dehydrating
	agents.
	B.     Carboxylic Acid Derivatives
	Structure and nomenclature of acid chlorides, esters, amides (urea) and acid 	anyhydrides.
	Relative stability of acyl derivatives, Physical properties, interconversion of acid 	derivatives by nucleophilic acyl substitution.
	Preparation of carboxylic acid derivatives, chemical reaction. Mechanism of 	esterification and hydrolysis (acidic and basic)
	C.    Organic Compounds of Nitrogen
	Preparation of nitroalkanes and nitroarenes, Chemical reactions of nitroalkanes. 	Mechanism of nucleophlic substitution in nitroarenes and their reductions in acidic, 	neutral and alkaline media, Picric acid.
	Halonitroarenes reactivity, Structure and nomenclature of amines, physical properties, 	Stereochemistry of amines, Separation of a mixture of primary, secondary and tertiary 	amines. Structural features effecting basicity of amines. Amine salts as phase-transfer 	catalysts, Preparation of alkyl and aryl amines (reduction of nitro compounds, nitriles), 	reductive amination of aldehydic and ketonic compounds, Gabriel-phthalimide reaction, 	Hofmann bromamide reaction. Reactions of amines, electrophilic aromatic substituton in 	aryl amines, reactions of amines with nitrous acid. Synthetic transformations of 	aryldiazonium salts, azo coupling.
B.Sc.-2 
Chemistry 
Paper-Ill 
Physical Chemistry
M.M. 50                                                                                                                        Duration-3.00 hours
Unit-I
	Thermodynamics & Chemical Equilibrium
	Thermodynamics -1
	Definitions of thermodynamic terms 
	System, surroundings, Types of systems, intensive and extensive properties, State and 	path functions and their differentials, Thermodynamic processes, concept of heat and 	work.
	First Law of Thermodynamics 
	Statement, definition of internal energy and enthalpy, Heat capacity, heat capacities at 	constant volume and pressure and their relationship, Joule's law Joule-Thomson 	coefficient and inversion temperature. Calculation of w, q, dU & dH for the 	expansion of ideal gases under isotheral and adiabatic conditions for reversible 	process.
	Thermochemistry
	Standard state, standard enthalpy of formation - Hess's Law of heat summation and its 	applications, Heat of reaction at constant pressure and at constant volume, Enthalpy 	of neutralization, Bond dissociation energy and its calculation from thermo-chernical 	data, temperature dependence of enthalpy, Kirchhoffs equation.
Unit-II
	A.  Chemical Equilibrium
	Equilibrium constant and free energy, Thermodynamic derivation of law of mass
	action, Le Chatelier's principle
	Reaction isotherm and reaction isochore - Clapeyron-Clausius equation and its
	applications.
	Thermodynamics-II
	B. Second Law of Thermodynamics 
	Need for the law, different statements of the law, Cornet's cycle and its efficiency, 	Carnot's theorem. Thermodynamic scale of temperature.
	Concept of entropy
	Entropy as a state function, entropy as a function of V & T, entropy as a function of P 	& T, entropy change in physical change, Clausius inequality, entropy as a criteria of 	spontaneity and equilibrium, Entropy change in ideal gases and mixing of gases.
	Gibbs and Helmholtz functions
	Gibbs function (G) and Helmhotz function (A) as thermodynamic quantities, A & G 	as criteria for thermodynamic equilibrium and spontaneity, their advantage over 	entropy change, Variation of G and A with P, V and T.
	C- Third Law of Thermodynamics
	Nernst heat theorem, statement and concept of residual entropy. Nernst distribution 	law - thermodynamic derivation, applications.
Unit-III
	Electrochemistry-I & Solutions
	A. Electrochemistry - I
	Electrical transport- Conduction in metals and in electrolyte solutions, specific 	conductance molar and equivalent conductance, measurement of equivalent 	conductance, variation of molar equivalent and specific conductance with dilution.
	Migration of ions and Kohlrausch's law, Arrhenius theory of electrolyte dissociation 	and its limitations, weak and strong electrolytes, Ostwald's dilution law its uses and 	limitations, Debye-Huckel-Onsager's equation for strong electrolytes (elementary 	treatment only), Transport number, definition and determination by Hittorf s method 	and moving boundary method.
	Applications of conductivity measurements; determination of degree of dissociation, 	determination of Ka of acids, determination of solubility product of a sparingly 	soluble salt, conductometric titrations.
	B.    Solutions
	Liquid - Liquid mixtures- Ideal liquid mixtures, Raoult's and Henry's law, Non-ideal 	system-azeotropes - HcI-H2O and ethanol - water systems.
	Partially miscible liquids- Phenol - water, trimethylarnine - water, nicotine-water 	systems, Immiscible liquids, steam distillation.
Unit-IV
	Electrochemistry- II & Phase
	A.       Electrochemistry- II
	Types of reversible electrodes - gas-metal ion, metal-ion, metal-insoluble salt-anicn 	and redox electrodes, Electrode reactions, Nernst equation, derivation of cell E.M.F. 	and single electrode potential, strandard hydrogen electrode- reference electrodes and 	their applications, standard electrode potential, sign conventions, electrochemical 	series and its significance.
	Electrolytic and Galvanic cells-reversible and irreversible cells, conventional 	representation of electrochemical cells;
	EMF of a cell and its measurements, Computation of cell EMF, Calculation of 	thermodynamic quantities of cell reactions ((G, (H and K)
	Concentration cell with and without transport, liquid junction potential, application of 	concentration cells, valency of ions, solubility product and activity coefficient, 	potentiometric titrations.
	Definition of pH and pKa, determination of pH using hydrogen, quinhydrone and 	glass electrodes, by potentiometric methods;
	Buffers - Mechanism of buffer action, Henderson-Hassel balch- equation, application
	of  buffer solution, Hydrolysis of salts
	(B) Phase Equilibrium
	Statement and meaning of the terms-phase, component and degree of freedom, 	derivation of Gibb's phase rule, phase equilibria of one component system-water, 	'CO2' and 'S' systems
	Phase equilibria of two component system - solid liquid equilibria simple eutectic - 	Bi-Cd, Pb-Ag systems, desilverisation of lead.
	Solid solutions - Compound formation with congruent melting point (Mg-Zn) and 	incongruent melting point, (FeCl3-H2O) and (CuSO4-H2O) systems.
B.Sc.-2
 Practical 
180 hours. (6 hours/week)
M.M. 50                                                                                                                        
	Inorganic Chemistry 
	Calibration of fractional weights, pipettes and burettes, Preparation of standards 	solutions, Dilution - 0.1 M to 0.001 M solutions.
	Quantitative Analysis								10
	Volumetric Analysis 
	(a)      Determination of acetic acid in commercial vinegar using NaOH.
	(b)      Determination of alkali content- antacid tablet using HCI.
	      (c)  Estimation of calcium content in chalk as calcium oxalate by permanganometry.
	(d)       Estimation of hardness of water by EDTA. V
	(e)       Estimation of ferrous and ferric by dichromate method.
	(f)        Estimation of copper using thiosulphate. Gravimetric Analysis 
	Gravimetric analysis								10
	Estimation of Cu as CuSCN and Ni as Nickel dimenthyl glyoxime, 

	Organic Chemistry 							10
	Laboratory Techniques
	A.     Thin Layer Chromatography
        	  Determination of Rf values and identification of organic compounds
	(a)    Separation of green leaf pigments (spinach leaves may be used).
	 (b)  Preparation of separation of 2, 4-dinitrophenylhydrazones of acetone, 2~ butanone,        	hexan-2, and 3-one using toluene and light petroleum (4060)
	(c)      Separation of a mixture of dyes using cyclohexane and ethyl acetate (8.5  1.5)
	B. Paper Chromatography 
	Ascending and Circular Determination of R/ values and identification of organic compounds
	(a)      Separation of a mixture of phenylalanine and glycine, Alanine and aspartic acid, Leucine and glutamic acid, Spray reagent - ninhydrin.
	(b)      Separation of a mixture of D, L - alanine, glycine, and L-Leucine using n-butanolicacetic acidwater (415), Spray reagent - ninhydrin.
	(c)    Separation of monosaccharide - a mixture of D-galactose and D-fructose using n-butanolacetonewater (451), spray reagent - aniline hydrogen phthalate.
	Qualitative Analysis
	Identification of an organic compound through the functional group analysis, 	determination of melting point and preparation of suitable derivatives. 	   10
	Physical Chemistry 
	Transition Temperature
	1.  Determination of the transition temperature of the given substance by thermometric 	/dilatometric method (e.g. nCl2.4H2O/SrBr2.2H2O).
	Phase Equilibrium
	2. To study the effect of a solute (e.g. NaCI, succinic acid) on the critical solution temperature of two partially miscible liquids (e.g. phenol-water system) and to determine the concentration of that solute in the given phenol-water system.
	3.  To construct the phase diagram of two component (e.g. dlphenylamine -benzophenone) system by cooling curve method.
	Thermochemistry
	1.   To determine the solubility of benzoic acid at different temperatures and to determine (H of the dissolution process.
	2. To determine the enthalpy of neutralization of a weak acid/weak base versus strong base/strong acid and determine the entrhalpy of ionization of the weak acid/weak base.
	3.   To determine the enthalpy of solution of solid calcium chloride and calculate the lattice energy of calcium chloride from its enthalpy data using using Born - Haber Cycle.
Viva-Voce � 05
Practical Record - 05


B.Sc.-3 
Chemistry 
Paper-I
Inorganic Chemistry 
M.M. 75                                                                                                                        Duration-3.00 hours
Unit-I
	A.         Metal-ligand bonding in Transition Metal Complexes
	Limitations of valance bond theory, an elementary idea of crystal field theory, crystal 	field splitting in octahedral, tetrahedral and square planner complexes, factors 	affecting the crystal-field parameters.
	B.       Thermodynamic and Kinetic Aspects of Metal Complexes
	A brief outline of thermodynamics stability of metal complexes and factors affecting 	the stability, stability constants of complexes and their determination, substitution 	reactions of square planar complexes.
Unit -II
	A.       Magnetic Properties of Transition Metal Complexes
	Types of magnetic behaviour methods of determining magnetic susceptibility, spin-	only formula, L-S coupling, correlation of ms and meff values, orbital contribution to 	magnetic moments, application of magnetic moment data for 3d-metal complexes.
	B.       Electronic spectra of Transition Metal Complexes
	Types of electronic transitions, selection rules for d-d transitions, spectroscopic 	ground states, spectrochemical series, Orgel-energy level diagram for d1 and d9 states, 	discussion of the electronic spectrum of [Ti(H2O)6]3+ complexion.
Unit -III
	A.       Organometallic Chemistry
	Definition, nomenclature and classification of organometallic compounds,
	Preparation, properties, bonding and applications of alkyls and aryls of Li, Al, Hg, Sn.
	Metal carbonyls 18 electron rule, preparation, structure and nature of bonding in the 	mononuclear carbonyls.
	B.       Silicones and Phosphazenes
	Silicones and phosphazenes as examples of inorganic polymers, nature of bonding in 	triphosphazenes.


Unit-IV
	A.     Hard and Soft Acids and Bases (HSAB)
	Classification of acids and bases as hard and soft, Pearson's HSAB concept, acid-base 	strength and hardness and softness, Symbiosis, theoretical basis of hardness and 	softness, electro negativity and hardness and softness.
	B.    Bioinorganic Chemistry
	Essential and trace elements in biological processes, metalloporphyrins with special 	reference to hemoglobin and myoglobin, Biological role of alkali and alkaline earth 	metal ions with special reference to Ca2+.
B.Sc.-3
 Chemistry 
Paper-II
Organic Chemistry 
M.M. 75                                                                                                                        Duration-3.00 hours
Unit-I
	Spectroscopy
	Nuclear magnetic resonance (NMR) spectroscopy, Proton magnetic resonance (1H 	NMR) spectroscopy, nuclear shielding and deshielding, chemical shift and molecular 	structure, spin-spin splitting and coupling constants, areas of signals, interpretation of 	1H NMR spectra of simple organic molecules such as ethyl bromide, ethanol, 	acetaldehyde, 1,1, 2-tribromoethane, ethyl acetate, toluene and acetophenone, 	Problems pertaining to the structures elucidation of simple organic compounds using 	UV, IR and 1H NMR spectroscopic, techniques.
Unit-II
	A. Organometallic Compounds
	Organomagnesium compounds  the Grignard reagents, formation, structure and chemical 	reactions.
	Organozinc compounds formation and chemical reactions. Organolithium compounds 	formation and chemical reactions.
	B.       Organosulphur Compounds
	Nomenclature, structural formation, methods of formation and chemical reactions of 	thiols, thioethers, sulphonic acids, sulphonamides and Sulphaguanidine.
	C.     Heterocyclic Compounds
	Introduction  Molecular orbital picture and aromatic characteristics of pyrrole, furan, 	thiophene and pyridine, Methods of synthesis and chemical reactions with particular 	emphasis on the mechanism of electrophilic substitution, Mechanism of nucleophilic 	substitution reaction in pyridine derivatives, Comparison of basicity of pyridine, piperidine 	and pyrrole.
	Introduction to condensed five and six membered heterocycles, Preparation and reactions 	of indole, quinoline and isoquinoline with special reference to Fisher indole synthesis, 	Skraup synthesis and Bischler-Nepieralski synthesis, Mechanism of electrophilc 	substitution reactions of indole, quinoline and isoquinoline.
Unit-III
	A.       Carbohydrates
	Classification and nomenclature, Monosaccharides, mechanism of osazone formation, 	interconversion of glucose and fructose, chain lengthening and chain shortening of 	aldoses. Configuration of monosaccharides, Erythro and threo diastereomers, Conversion 	of glucose intro mannose, Formation of glycosides, ethers and esters, Determination of 	ring size of monosaccharides, Cyclic structure of D(+)-glucose, Mechanism of 	mutarotation.
	Structures of ribose and deoxyribose, An introduction to disaccharides (maltose, sucrose 	and lactose) and polysaccharides (starch and cellulose) without involving structure 	determination.
	B.      Amino Acids, Peptides, Proteins and Nucleic Acids
	Classification, structure and stereochemistry of amino acids, Acid-base behaviour 	isoelectric point and electrophoresis, Preparation and reactions of (-amino acids, 	Structure and nomenclature of peptides and proteins, Classification of proteins, peptide 	structure determination, end group analysis, selective hydrolysis of peptides, classical 	peptide synthesis, solid-phase peptide synthesis, Structures of peptides and proteins, 	Levels of protein structure, Protein denaturation/ renaturation;
	Nucleic acids  Introduction, constituents of nucleic acids, Ribonucleosides and 	ribonucleotides, The double helical structure of DNA.
Unit-IV
	A.       Fats, Oils and Detergents
	Natural fats, edible and industrial oils of vegetable origin, common fatty acids, 	glycerides, hydrogenation of unsaturated oils, Saponification value, iodine value, acid 	value, Soaps, synthetic detergents, alkyl and aryl sulphonates.
	B.    Synthetic Polymers
	Addition or chain-growth polymerization, Free radical vinyl polymerization, ionic 	vinyl polymerization, Ziegler-Natta polymerization and vinyl polymers,
	Condensation or step growth-polymerization, Polyesters, plyamides, phenol 		formaldehyde resins, urea formaldehyde resins, epoxy resins and polyurethanes, 	Natural and synthetic rubbers, Elementary idea of organic conducting polymers.
	C.      Synthetic Dyes
	Colour and constitution (electronic Concept), Classification of dyes, Chemistry and 	synthesis of Methyl orange, Congo red, Malachite green, crystal violet, 	phenolphthalein, fluorescein, Alizarin and Indigo.
	D.        Organic Synthesis via Enolates
	Acidity of (-hydrogens, alkylation of diethyl malonate and ethyl acetoacetate, 	Synthesis of ethyl acetoacetate the Claisen condensation, Keto-enol tautomerism of 	ethyl acetoacetate.
	Alkylation of 1, 3-dithianes, Alkylation and acylation of enamines.
B.Sc.-3
 Chemistry 
Paper-Ill
 Physical Chemistry 
M.M. 75                                                                                                                        Duration-3.00 hours
Unit-I
          A.         Introductory Quantum Mechanics
	Black-body radiation, Planck's radiation law, photoelectric effect, heat capacity of solids, 	Bohr's model of hydrogen atom (without derivation) and its defects, Compton effect, de-	Broglie's hypothesis, the Heisenberg's uncertainty principle, Hamiltonian Operator.
	B.        Spectroscopy
	Introduction  electromagnetic radiation, regions of the spectrum, basic features of 	different spectrophotometers, statement of the born-oppenheimer approximation, 	degrees of freedom.
            C.       Physical Properties and Molecular Structure
	Optical activity, polarization - (Clausius - Mossotti equation), orientation of dipoles in an 	electric field, dipole moment, induced dipole moment, measurement of dipole moment-	temperature method and refractivity method, dipole moment and structure of molecules, 	magnetic properties-paramagnetism, diamagnetism and ferromagnetic, Magnetic 	susceptibility, its measurements and its importance.



Unit-II
	Elementary Quantum Mechanics
Schrodinger wave equation and its importance, physical interpretation of the wave function, postulates of quantum mechanics, particle in a one dimensional box.
Schrodinger wave equation for H-atom, separation into three equations (without derivation), quantum numbers and their importance, hydrogen like wave functions, radial wave functions, angular wave functions.
Molecular orbital theory, basic ideas - criteria for forming M.O. from A.O., construction of M.O's by LCAO - H2+ ion, calculation of energy levels from wave functions, physical picture of bonding and anti-bonding wave functions, concept of a, a*, n, n* orbitals and their characteristics, Hybrid orbitals - sp, sp3, sp2, calculation of coefficients of A.O's used in sp and sp2 hybrid orbitals and interpretation of geometry.
Introduction to valence bond model of H2, comparison of M.O. and V.B. models.
Unit-III
A. Rotational Spectrum
Diatomic Molecules 
Energy levels of a rigid rotor (semi-classical principles), selection rules, spectral intensity, distribution using population distribution (Maxwell-Boltzmann distribution) determination of bond length, qualitative description of non-rigid rotor, isotope effect.
(B) Vibrational Spectrum 
Infrared Spectrum Energy levels of simple harmonic oscillator, selection rules, pure vibrational spectrum, intensity, determination of force constant and qualitative relation of force constant and bond energies, effect of anharmonic motion and isotope on the spectrum, idea of vibrational frequencies of different functional groups.
(C) Raman Spectrum  Concept of polarizability, pure rotational and pure vibrational Raman spectra of diatomic molecules, selection rules.
(E) Electronic Spectrum  Concept of potential energy curves for bonding and antibonding molecular orbitals, qualitative description of selection rules and Franck-Condon principle.
Qualitative description ( ( ( M.O. their energy levels and the respective transitions.
Unit-IV
Photochemistry. Solutions. Dilute Solutions and Colligative Properties
(A).      Photochemistry
Interaction of radiation with matter, difference between thermal and photochemical processes, Laws of photochemistry Grotthus - Draper law, Stark - Einstein law, Jablonski diagram depicting various processes occurring in the excited state, qualitative description of fluorescence, phosphorescence, non- radiative processes (internal conversion, intersystem crossing), quantum yield, photosensitized reactions - energy transfer processes (simple examples), Kinetics of Photo chemical reaction.
(B) Solutions, Dilute Solutions and Colligative Properties
Ideal and non-ideal solutions, methods of expressing concentrations of solutions, activity and activity coefficient.
Dilute solution, colligative properties, Raoult's law, relative lowering of vapour pressure, molecular weight determination, Osmosis, law of osmotic pressure and its measurement, determination of molecular weight from osmotic pressure, Elevation of boiling point and depression of freezing, Thermodynamic derivation of relation between molecular weight and elevation in boiling point and depression in freezing point. Experimental methods for determining various colligative properties.
Abnormal molar mass, Van't Hoff factor, Colligative properties, degree of dissociation and association of solutes.
B.Sc.-3
PRACTICAL
180 hrs. (12 hrs./weak)
M.M. 75                                                                                                                        
Inorganic Chemistry 
Synthesis and Analysis		                                          10			
 (a)  Preparation of sodium trioxalato ferrate (III),  Na3[Fe(C2O4)3] and determination of its composition by permagonometry.
(b)      Preparation of Ni-DMG complex, [Ni(DMG)2] Preparation of Tetramine Cu  
            (II) [(Cu(NH3)4]SO4 Complex.
 (d)      Preparation of cis-and trans-bis (oxalato) diaqua chromate (III) ion.
Instrumentation     	10						                                          
Colorimetry
(a) Job's method 
(b) Mole-ratio method - Adulteration - Food stuffs. Effluent analysis, water analysis
Solvent Extraction
Separation and estimation of Mg(ll) and Fe(ll) 
Ion Exchange Method
Separation and estimation of Mg(ll) and Zn(ll)
Organic Chemistry                                                                                                                            
Laboratory Techniques 
Steam Distillation
Naphtalene from its suspension in water
Clove oil from cloves
Separation of o-and p-nitrophenols
Column Chromatography		05					                               
Separation of fluorescein and methylene blue, Separation of leaf pigments from spinach leaves Resolution of racemic mixture of (+) mandelic acid
Analysis	                   10								Analysis of an organic mixture containing two solid components
using water, NaHCO3,
NaOH for separation and preparation of suitable derivatives
Synthesis of Organic Compounds	05					                               
a)  Acetylation of salicylic acid, aniline, glucose and hydroquinone, Benzoylation 
       of aniline and phenol
(b)  Aliphatic electrophlic substitution
        Preparation of iodoform from ethanol and acetone
(c)  Aromatic elutrophilic substitution Nitration
        Preparation of m-dinitrobenzene
Preparation of p-nitroacetanilide
Halogenation - Preparation of p-bromoacetanilide, Preparation of 2, 4, 6 tribromophenol.
(d)  Diazotization/coupling
        Preparation of methyl orange and methyl red
(e)   Oxidation
        Preparation of benzoic acid from toluene
(f)    Reduction
        Preparation of aniline from nitrobenzene, Preparation of m-nitroaniline from m-
     dinitrobenzene
Stereochemical Study of Organic Compounds via Models
R and S configuration of optical isomers
E, Z configuration of geometrical isomers
Conformational     analysis    of    cyclohexanes    and    substituted
cyclohexanes
Physical Chemistry 							                                           20
Electrochemistry 
1. To determine the strength of the given acid conductometrically using standard alkali solution.
2. to determine the solubility and solubility product of a sparingly soluble electrolyte conducomeirically.
3.  to study the saponification of ethyl acetate condutornetricaiiy.
4. To determine the ionization constant of a weak acid condutornetricaiiy.
5.  To   titrate   potentiometrically  the   given   ferrous   ammonium   sulphate solution using KMnO4/K2Cr2O7 as titrant and calculate the redox potential of Fe++/Fe+++ system on the hydrogen scale. 
Refractromeiry, Polarimetry
1.  To verify law of refraction of mixtures (e.g. of glycerol and water) using Abbe's refractometer.
2.  To determine the specific rotation of a given optically active compound.
3.  To determine stoichiometry and stability constant of complexes.
Molecular Weight Determination
1. Determination of molecular weight of a non-volatile solute by Rast method/ Beckmann freezing point method.
2.  Determination of the apparent degree of dissociation of an electrolyte (e.g., NaCl) in aqueous solution at different concentrations by ebullioscopy.
Colorimetry
To verify Beer - Lambert Law for KMnO4/K2Cr2O7 and determining the
concentration of the given solution of the substance from absorption measurement.
Viva-voce � 08
Practical Record - 07








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